Khattab, T., Rehan, M. (2018). Synthesis and Characterization of Bis-azo 1,2,4,5-Tetrazine Dyestuff. Journal of Textiles, Coloration and Polymer Science, 15(1), 33-36. doi: 10.21608/jtcps.2018.5033.1003
Tawfik A. Khattab; Mohamed Rehan. "Synthesis and Characterization of Bis-azo 1,2,4,5-Tetrazine Dyestuff". Journal of Textiles, Coloration and Polymer Science, 15, 1, 2018, 33-36. doi: 10.21608/jtcps.2018.5033.1003
Khattab, T., Rehan, M. (2018). 'Synthesis and Characterization of Bis-azo 1,2,4,5-Tetrazine Dyestuff', Journal of Textiles, Coloration and Polymer Science, 15(1), pp. 33-36. doi: 10.21608/jtcps.2018.5033.1003
Khattab, T., Rehan, M. Synthesis and Characterization of Bis-azo 1,2,4,5-Tetrazine Dyestuff. Journal of Textiles, Coloration and Polymer Science, 2018; 15(1): 33-36. doi: 10.21608/jtcps.2018.5033.1003
Synthesis and Characterization of Bis-azo 1,2,4,5-Tetrazine Dyestuff
Receive Date: 04 September 2018,
Accept Date: 26 September 2018
Abstract
The design, synthesis and characterization of symmetrical 3,6-Bis(2-(4-(dodecyloxy)phenyl)-1-(4-(phenyl)diazene)-1,2,4,5-tetrazine are described. The novel sym-tetrazine was prepared by addition reaction of 4-(2-(4-decyloxyphenyl)diazenyl)benzonitrile with hydrazine monohydrate followed by oxidation reaction to afford the corresponding bis(azo)-1,2,4,5-tetrazine. The chemical structure of the sym-tetrazine compound was confirmed by elemental analysis, fourier-transform infrared spectroscopy (FT-IR), and nuclear magnetic resonance (1H and 13C NMR) spectral measurements. The design, synthesis and characterization of symmetrical 3,6-Bis(2-(4-(dodecyloxy)phenyl)-1-(4-(phenyl)diazene)-1,2,4,5-tetrazine are described. The novel sym-tetrazine was prepared by addition reaction of 4-(2-(4-decyloxyphenyl)diazenyl)benzonitrile with hydrazine monohydrate followed by oxidation reaction to afford the corresponding bis(azo)-1,2,4,5-tetrazine. The chemical structure of the sym-tetrazine compound was confirmed by elemental analysis, fourier-transform infrared spectroscopy (FT-IR), and nuclear magnetic resonance (1H and 13C NMR) spectral measurements.
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